| MS Comment of details
|
[column] InertSustain AQ-C18 (1.5 x 50 mm, … [column] InertSustain AQ-C18 (1.5 x 50 mm, 3 micrometer; GL Sciences)
[gradient] Solvent A: water containing 0.1% v/v formic acid; Solvent B: acetonitrile; Gradient 2% B (0 min), 2% B (1.5 min), 98% B (13.5 min), 98% B (17 min), 2% B (17.01 min), and 2% B (18.5 min)
[total separation time] 18.5 min 8.5 min)
[total separation time] 18.5 min
|
| MS Description
|
Compound extraction and LC-MS measurement were performed as same as described in the ESI positive mode (MS01, http://metabolonote.kazusa.or.jp/SE229:/MS01) except for modifications below: polarity, negative; MS/MS Collision energy.
|
| MS ID
|
MS11 +
|
| MS Instrument
|
Nexera X2 (Shimadzu), Compact (Bruker Daltonics) +
|
| MS Instrument Type
|
LC-QTOF-MS +
|
| MS Ion Mode
|
Negative +
|
| MS Ionization
|
ESI +
|
| MS Title
|
LC-Q-Tof-MS, ESI, Negative +
|
| Modification dateThis property is a special property in this wiki.
|
7 February 2024 07:09:15 +
|
